ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Streicher Test). ASTM A practice – Free download as Excel Spreadsheet .xls /.xlsx), PDF File .pdf), Text File .txt) or read online for free. ASTM A Practice B test. In this test a sample of surface area cm. 2 is exposed for a period of hours to boiling solution of 50% H2SO4 + %.
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Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
Rockwell a2262 Superficial Hardness. Please refer to the specification for more details. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. If the structure is acceptable no additional testing is required.
Intergranular corrosion shows satm as the dark black lines around the grain boundaries. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. Based on your materials, application, and requirements, the other 4 methods provide specific focuses. It depends on which Practice is selected, but typically ranges from to days for different tests. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Historical Version s – view previous versions of standard.
Contact us now for pricing or a quote! Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
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Intergranular Attack – ASTM A – Colorado-Metallurgical-Services
The level of corrosion is determined x262 mass loss. ASTM A testing is a popular method of choice due to practjce variety of practices available and the relatively short turnaround for results.
This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. If you are not sure, please asfm us for assistance.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. Practice B, also known as s262 Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. Plating and Coating Testing.
Carbon and Sulfur Analysis. The inch-pound equivalents are in parentheses and may be approximate. Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. These tests do not provide a basis for practtice resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.
How do you select the right ASTM corrosion testing method for your material? This method is preferable for chromium depletions and corrosion in intermetallic phases. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use.
For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.
Discover perspectives, resources, and advice from our world-leading Engaged Experts. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation. The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.
The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. This specification is for detecting susceptibility to intergranular attack IGA. A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
Wilson Hardness Conversion Chart. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack.
A recent publication on intergranular corrosion.