E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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Energy of this wavelength is absorbed as the gas passes through a cell body in which the IR energy is transmitted. In the absence of CO and CO2, the energy received by each detector is maximum.
NOTE 4—Repeat the calibration when: Individual reprints single or multiple copies of this standard f1019 be obtained by contacting ASTM at the above address or at phonefaxor service astm. Prepare more capsules of sulfur solution B if necessary. Price-list Explanations X-ray fluorescents and combustion technology are used for the analyses: NOTE 23—If the unit does not have this function, the blank value must be subtracted from the total result prior to any calculation.
Use Calibrant C as the primary calibrant and analyze at least three specimens to determine the calibration slope. Remove from the furnace and cool in air for 90 6 15 s before use.
E — 03 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, asfm Cobalt Alloys1 This standard is issued under the xed designation E ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision.
Comment 1 g sample 1 g sample. Users of this test method are cautioned that use of it above 0. Use Calibrant CCC as the primary calibrant and analyze at least ast test samples to determine the calibration slope.
The detector response data are processed and displayed directly as percent oxygen. The oxygen combines with carbon from the crucible to form carbon monoxide CO and is carried by the owing inert gas stream to either a thermal conductivity or an infrared detector. Add to Alert PDF. This mechanism will electronically compensate for the blank value. NOTE 15—If the unit does not have this function, the average blank value must be subtracted from the DVM readings for reference materials and specimens Note If they are not within 0.
The detector output is compared to that obtained from similar certied reference materials and is displayed as oxygen content of the sample.
One asttm is used as both a reference and a measure chamber. NOTE 22—The uncertainty of results obtained using this test method is dependent on the uncertainty of the values assigned to the calibration reference materials.
If necessary, wash three times with acetone by decantation to remove organic contaminants and dry at room temperature.
However, recognizing that commercial oxygen determinators are capable of handling higher concentrations, it may be that this test method can be used for oxygen concentrations outside of the scope.
The value should be within the allowable limits of the certied value. Part of the IR energy is absorbed by the SO2 present in the measure chamber while none is absorbed passing through the reference chamber. Using a clean le or water cooled silicon carbide grinding media, abrade all surfaces of the sample to remove all traces of surface oxidation or other impurities, rinse in acetone, air-dry, and weigh.
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The nitrogen is separated from other liberated gases such as hydrogen and carbon monoxide and is nally measured in a thermal conductivity cell. Your Alert Profile lists the documents that will be monitored. NOTE 1—The accelerator should contain no more than 0. Please first verify your email before subscribing to alerts. Dilute to volume and mix. Turn on the instrument and allow sufficient warm up time to stabilize the system.
Adjust the d1019 to provide a reading within NOTE 2—The uncertainty of results obtained using this test method is dependent on the uncertainty of the values assigned to the calibration reference materials. Link to Active This link will always route to the current Active version of the standard.